Expanded Laser Beam for Online Measurement of Dispersed Phase Holdup in Agitated Flow Liquid-Liquid Mixer of Pilot Plant Scale | AIChE

Expanded Laser Beam for Online Measurement of Dispersed Phase Holdup in Agitated Flow Liquid-Liquid Mixer of Pilot Plant Scale

Type

Conference Presentation

Conference Type

AIChE Spring Meeting and Global Congress on Process Safety

Presentation Date

April 20, 2021

Duration

20 minutes

Skill Level

Intermediate

PDHs

0.50

Laser transmission Technique (LTT) where a laser beam is used in conjunction with a beam, that is expanded enough to cover the average droplet size of the dispersed liquid in a liquid-liquid mixture has been applied for continuous measurement of the droplet phase volume fraction in agitated flow mixer of a pilot plant scale. The nature of difficulties inherent with the online measurement of the droplet phase holdup in an environment free of hydrodynamic disturbance when a wave of light is transmitted through the dispersion path of the liquid mixture are discussed. This study reports the first data for continuous measurements of dispersed phase holdup for a pilot plant scale liquid-liquid mixer of commercial design, where the measurements have no limitations to the geometrical aspects. Experimental results from a cubic mixing tank with dispersion depth of 30 cm were recorded. Online measurements were carried out in the presence of revolving impeller and transmission of a laser beam. The volume of the liquid-liquid mixer was 20.42 liter and the successfully measured dispersed phase holdup was ranged between 0.15-0.75. In this work, the arrangement of the laser setup was made to scan and measure the average liquid-liquid mixer holdup in the pilot plant scale of flow agitated liquid-liquid mixer. Thus, the LTT measurements was validated by comparing its results with that obtained from the liquid-liquid mixer shut-down procedure. In addition, the variation of the local holdup of the dispersed phase measured by LTT along the liquid-liquid mixer height has been studied and will be discussed.

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