Chemical Engineering Practice

Applying Mass and Energy Balances to Spray Drying

December
2009
Back To Basics
Tim Langrish
Mass and energy balances are not just for process and equipment design. They can also be used to improve dryer operations by answering various “what-if” questions about temperatures, flowrates, and moisture contents. <br><br>

High-Shear Mixers: Still Widely Misunderstood

November
2007
News Feature
Suzanne Shelley
Advanced modeling techniques and improved geometric features are helping designers and users of rotor-stator mixers to demystify these complex devices, and get more consistent predictable results.

Valves 101: Types, Materials, Selection

March
2009
Back To Basics
Brian Gordon
The most common valves used in chemical processing are ball valves, butterfly valves, diaphragm valves, and check valves.

Agitating Fibrous Materials

June
2010
Back To Basics
Gregory T. Benz
Slurry agitation involves complicated processes. This article presents guidelines for understanding the rheology of cellulosic and other fibrous materials, and outlines a method for scaling up their agitation.

Practical Process Control: Tuning and Troubleshooting

December, 2009
Practical Process Control (loop tuning and troubleshooting). This book differs from others on the market in several respects. First, the presentation is totally in the time domain (the word "LaPlace" is nowhere to be found). The focus of the book is actually troubleshooting, not tuning. If a...

Chemical Engineering Faculty Directory: 2009-2010

December, 2009
This faculty directory lists the contact information of all the faculty members, placement administrators, and student organizations of almost 500 worldwide universities and technical institutes offering chemical engineering curricula. This offers a comprehensive reference tool that is unique and...

Basic Process Measurements

June, 2009
A unique resource for process measurement Basic Process Measurements provides a unique resource explaining the industrial measuring devices that gauge such key variables as temperature, pressure, density, level, and flow. With an emphasis on the most commonly installed technologies, this guide...

Fluid Flow for the Practicing Chemical Engineer

June, 2009
This book teaches the fundamentals of fluid flow by including both theory and the applications of fluid flow in chemical engineering. It puts fluid flow in the context of other transport phenomena such as mass transfer and heat transfer, while covering the basics, from elementary flow mechanics to...

Thermodynamics for the Practicing Engineer

June, 2009
Thermodynamics for the Practicing Engineer, as the title suggests, is written for all practicing engineers and anyone studying to become one. Its focus therefore is on applications of thermodynamics, addressing both technical and pragmatic problems in the field. Readers are provided a solid base in...

Crystallization of Organic Compounds: An Industrial Perspective

May, 2009
Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of...

The Yoga of Process Development

AIChE Annual Meeting
Nov 17, 2008
Process Development is analogous to Yoga. It is a ‘Yoga' – a disciplined process for integrating the essential components to create a vision of the ‘...

Chemical Engineering Faculty Directory: 2006-2007

February, 2007
This one of a kind directory conveniently lists the contact information for chemical engineering faculty members, department heads, academic advisors, student organization advisors, and placement officers at over 450 Universities worldwide. The directory's easy-to-use format lists chemical...

Chemical Engineering Faculty Directory: 2005-2006

January, 2006
This faculty directory lists the contact information of all the faculty members, placement administrators, and student organizations of almost 500 worldwide universities and technical institutes offering chemical engineering curricula.

Spray Dryers: A Guide to Performance Evaluation, 2nd Edition

August, 2004
Spray Dryers: A Guide to Performance Evaluation, Second Edition discusses the reasons for spray drying. These reasons are usually to produce a product with certain desired properties or with better efficiency than other methods. The book discusses how to plan in light of these objectives and gives...

AIChE Equipment Testing Procedure - Particle Size Classifiers, 2nd Edition

June, 1993
This procedure offers complete methodologies for sampling and measuring particle streams and summarizes methods of particle size analysis. It also lists operating variables to be considered and measured. Although the procedure is intended specifically for particle classification equipment, many of...

Optimize Energy Use in Distillation

March
2012
Reactions and Separations
Douglas C. White
Nonlinearities in the response of a column to changes in operating conditions and in common economic valuation functions can have significant impacts on the economic optimum energy consumption for the column. Here’s a way to account for such...

The Case for Double Mechanical Seals

June
2009
Back To Basics
Jack Berg
Using double mechanical seals as part of thermoplastic pumps can prevent costly downtime and environmental damage.

The Chemical Industry Phoenix

June
2012
Process Automation Corner
Terry McMahon
Seven years ago, I wrote a column for another publica­ tion entitled “The U.S. Chemical Industry: R.I.P.” This pillar of American economic strength, which a few years earlier was the leading exporter among U.S. manufac­turing sectors (with net exports of $15–20 billion annually), was shriveling due in large part to policy blunders and regula­tory mistakes.

Harness Electricity to Operate Valves

June
2012
Back To Basics
Justin Ledger
Actuators automate valves by converting an input signal into motion. This article explains the basics of electric actuator design and explores the different types of electric actuators.

Reduce Unplanned Shutdowns

September
2003
Instrumentation
Cindy Scott
Today's intelligent devices are equipped with modern alarm technology that enables speedy delivery of critical information to key personnel, thus enhancing efficiency and minimizing downtime.

Physical and Chemical Equilibrium for Chemical Engineers

April, 2012
This book concentrates on the topic of physical and chemical equilibrium. Using the simplest mathematics along with numerous numerical examples it accurately and rigorously covers physical and chemical equilibrium in depth and detail. It continues to cover the topics found in the first edition...

Take Another Look at Steam Traps

June
2001
Fluids and Solids Handling
S. Raghavi  Chari
Think twice before installing a steam trap. In the case of superheated lines, steam traps may prove to be a waste of time, effort, and money

Troubleshooting Tangential Flow Filtration

June
2003
Reactions and Separations
Kent Iverson
Tangential flow filtration (TFF) is commonly used to concentrate and dialyze solutes. It generally involves the circulation of the feed solution over a filter surface. This article presents a brief overview of the principles governing TFF, and...

Efficient Technology Evaluation

February
2007
Critical Issues
Francesco Citro, Reuel Shinnar
To stay competitive in today's economic climate, rapid and effective assessments of new technologies is a must. Requiring a minimal amount of data, this powerful method can effectively evaluate new ideas and research programs at an early stage...

Choose the Right Elastomer

June
2008
Materials
William M. Stahl
Match a material's performance to process conditions to reduce leaks, improve safety and extend the mean time between failures (MTBF).

Improve Flange Joint Reliability

January
2011
Back To Basics
John Ludman, Mike Emery, Thomas Sandbrook
Proper design, installation, and maintenance of flanged connection systems can prevent loss of containment and process interruptions. Follow this seven-step approach to ensure reliability of this critical process equipment.

Inhibiting and Monitoring Corrosion

March
2012
Heat Transfer
Gary Geiger, Mel J. Esmacher, P.E.
Understand corrosion and ways to control it, and implement these monitoring techniques to improve cooling water system efficiency and reliability and reduce energy consumption.

Optimize Pipeline Design for Non-Newtonian Fluids

March
2002
Fluids and Solids Handling
Alejandro Anaya Durand, Cinthya Alejandra Anguilar Guerrero,  Edgar Amaro  Ronces
Use this graphical method to determine pipe diameter, fluid temperature and pressure drop for laminar and turbulent flow.

Evaluating Dryers for New Services

December
2003
Heat Transfer
Charles G. Moyers
Continuous dryers are accurately and easily evaluated using laboratory-scale simulators combined with the specific drying rate approach.

Effectively Manage the Lifecycle of a Product

July
2007
Information Technology
Baha Korkmaz, Marty Martin
By incorporating the batch standards S88 and S95 into the entire product lifecycle, companies can optimize their processes and project management. This enables them to rapidly get their products to market — a critical factor in staying competitive.

Minimize Scale-Up Risk

March
2010
SBE Special Section
Bertil Stromberg, J. Brad Cort, Thomas Pschorn
Proven commercial-scale equipment already exists for many operations involved in producing biofuels from lignocellulosic feedstocks.

Reduce Piloting Time and Cost

July
2011
Process Development
David A. Berg, Michael T. Cleary
Pilot-scale experimentation is essential to establish a sound foundation for a new chemical processing unit. These best practices can reduce the time and cost involved in process development.

Uncovering the Realities of Simulation

May
2001
Computational Methods
Andrew  Vieler, Marco S. Satyr, Oscar  Santollani , Rajeev  Agarwal, Yau-Kun Li
Running sophisticated process simulations does not guarantee correct results. You need to understand the thermodynamic assumptions underlying the program and how to ensure proper applications.

Size Letdown Lines for Pressure Surges

November
2001
Fluids and Solids Handling
Gianni  Anci
A high-pressure gas flow in a letdown circuit can cause damage to piping and equipment. Here is how to design a system to avoid damage should a pressurized gas flow occur GianniAnci-

Implementing an EHS Management Information System

May
2004
Information Technology
Jill Barson Gilbert
Information technology issues are just as important as business and environmental, health and safety considerations. Follow these ten tips to deply an effective EMIS with a positive return on investment.

Eliminate Iteration from Flow Problems

March
2008
Fluids and Solids Handling
John D. Barry
This article introduces a novel approach to solving flow and pipe-sizing problems based on two new dimensionless quantities that are independent of line size and flow.

Predicting Emissivities of Combustion Gases

June
2009
Heat Transfer
Alireza Bahadori, Hari B. Vuthaluru
Use this new correlation, which employs easy-to-solve algebraic equations to estimate gas emissivities, to simplify the design and optimization of boilers, furnaces and other combustion equipment.

Learn to Effectively Operate and Maintain Pumps

December
2011
Back To Basics
Daniel Kernan
Centrifugal pumps play a central role in chemical processing. Proper pump operation and maintenance can improve a facility's productivity, reduce downtime, and trim costs.

Optimize Mixing by Selecting the Proper Baffles

February
2002
Fluids and Solids Handling
Julian B. Fasano, Kevin J. Myers, Mark F. Reeder
It is common knowledge that baffles promote better flow in an agitated vessel, but how to apply them and what kind to use take some ingenuity.

Profiting From Your Pumping System

September
2003
Fluids and Solids Handling
Aimee McKane  , Vestal Tutterow,  Don Casada
Identify ways to minimize the lifecycle costs of your pumping system

Improve Solids Handling During Thermal Drying

November
2004
Fluids and Solids Handling
Herman Purutyan, John W. Carson, Thomas G. Troxel
Follow these guidelines for ensuring the proper flow of slurries, pastes and wet powders to achieve a dried product with the desired characteristics.

Selecting and Using Bolted Head Closures

April
2007
Fluids and Solids Handling
John C. Birkmire, P.E.
Proper design, fabrication, assembly and operation of a pressure vessel closure are essential to ensuring product containment, integrity and quality.

Solving Phase Equilibrium Problems

September
2008
Reactions and Separations
James R. Reinhardt, Terrence L. Chambers
Use this optimization-based approach to analyze multi-component, multi-phase Equilibria.

Visualizing the McCabe-Thiele Diagram

December
2009
Reactions and Separations
Paul M. Mathias
Use this spreadsheet-based visualization and interactive analysis of the McCabe-Theile diagram to understand the foundations of distillation engineering. <br><br>

Identifying Corrosion and Its Causes

April
2011
Fluids and Solids Handling
Gary Geiger, Mel J. Esmacher, P.E.
An important first step in maintaining equipment reliability and efficiency is understanding the various types of corrosion damage that can occur.

Realize Greater Benefits from CFD

March
2001
Fluids and Solids Handling
Ahmad H. Haidari, Andre  Bakker,  Lanre M. Oshinowo
Computational fluid dynamics has moved from mainframes to PCs and laptops. Newer and better software lets you conduct analyses not possible before, and regular engineers, not just experts, can now carry out CFD.

Air Heater Cleaning Simplified

October
2001
Heat Transfer
Brad Buecker
This high-pressure water washing technique can be used to clean Ljungstrom-type air heaters.

Reduce Costs with Dividing-Wall Columns

May
2002
Reactions and Separations
Dennis O'Brien, Douglas A. Stewart, James W. Harris, Michael A. Schultz, Mohamed S.M. Shakur, Steven P. Rosenblum
These distillation columns can significantly reduce capital and energy expenses vs. conventional multicolumn arrangements.

Computationally Evaluate Self-Reactivity Hazards

February
2003
Reactions and Separations
Edward S. Shanley, Michelle R. Murphy, Surendra K. Singh
Here is a method that rates the tendency of new compounds to self-explode without the need to perform extensive laboratory tests.

Production Modeling for Multimodal Operations

February
2004
Information Technology
Jeffrey D. Kelly
Two new views for production modeling are introduced - production flow networks and production flow maps - that focus on unit operations and feedstocks, respectively.

Beware of Pitfalls of Carbon Dioxide Freezing Prediction

March
2005
Heat Transfer
Steve Chafin , Tim Eggeman
Carbon dioxide freezing in a cryogenic system can result in plugging and other operational problems. This article offers insights into the carbon dioxide freezing phenomenon.

Pipeline Pressure Drop: A New Design Correlation

June
2006
Fluids and Solids Handling
Roger Gilmont
A linear equation has been derived to accurately calculate the flowrate of fluids in the laminar and turbulent regions, and to derive an equation for use in the transitional regions.

Selecting Entrainers for Azeotropic Distillation

March
2009
Reactions and Separations
Lionel O’Young, Madhura Chiplunkar, Vivek Julka
This systematic methodology uses residue curve maps to identify and evaluate substances that can facilitate distillation by breaking an azeotrope.

Uncovering the Realities of Simulation, Part 2

June
2001
Computational Methods
Andrew  Vieler, Marco S. Satyro, Rajeev  Agarwal, Yau-Kun Li,  Oscar  Santollani
Simulation software is a commonly used design tool, thanks mainly to its availability on the desktop. However, one has to understand thermodynamic basics before accepting the desktop's final answer.

Real World Modeling of Distillation

July
2003
Reactions and Separations
Harry Kooijman, Rajamani Krishna , Ross Taylor
Previously, simulations based on nonequilibrium, or rate-based, models were considered impractical due to their complexity. However, with ever-increasing computing power, these simulations are not only feasible, but in some circumstances they should...

Clarifying Centrifuge Operation and Selection

August
2004
Fluids and Solids Handling
Victor Norton ,  William Wilkie
Before selecting a centrifuge for your application, understand its principles of operation and investigate the key process variables.

Integrate Process Simulation and Process Synthesis

October
2005
Computational Methods
Dominic Chwan Yee Foo, Michael Lynn McGuire, Murugan Selvan, Zainuddin Abdul Manan
The design of a new process using computer simulations to analyze a process flowsheet based on the onion model can save time, effort and, ultimately, money.

Effectively Control Column Pressure

January
2001
Reactions and Separations
Andrew W. Sloley 
Maintaining proper pressure can play a crucial role in the stable operation of a distillation column. Here’s how to select the most appropriate pressure-control scheme.
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