Process Design & Development

Design Reactors via CFD

December
2001
Reactions and Separations
Ahmad H. Haidari, Andre Bakker, Elizabeth M. Marshall
Using computational fluid dynamics to design commercial-size batch and continuous reactors can eliminate subjective experience and empiricism, leading to better-designed, more-efficient units.

How to Scale-Up Mixing Processes in Non-Newtonian Fluids

May
2003
Fluids and Solids Handling
Christopher Henry , Robert J. Wilkens,  Lew E. Gates
This article will describe the relationships that must be understood to scale-up fluid mixing processes in non-Newtonian, power-law fluids. The principles described apply to both close-clearance impellers, such as anchors and helixes, and to open...

Find Mixing Success Through Failures - Part 2

December
2008
Fluids and Solids Handling
David S. Dickey, Gary K. Patterson
Understanding when and why mixing fails in the laboratory is often the only way of avoiding a similar failure in a production-scale reactor. Here we examine mixing in stirred-tank reactors and provide guidance on scale-up.

Selecting Nickel Alloys for Corrosive Applications

May
2007
Materials
Paul Crook
Nickel and its alloys offer resistance to attack by a wide range of chemicals, including acids, alkalis and salts, making these materials suitable for may CPI applications.

Clarifying Centrifuge Operation and Selection

August
2004
Fluids and Solids Handling
Victor Norton ,  William Wilkie
Before selecting a centrifuge for your application, understand its principles of operation and investigate the key process variables.

Selecting Corrosion-Resistant Materials

December
2006
Materials
Francesco Picciotti, Marcello Picciotti
This article looks at some common corrosion-resistant alloys and gasket materials that are available for use in applications with high pressures and temperatures.

Bridge the Gap with Semicontinuous Distillation

August
2001
Reactions and Separations
James R. Phimister ,  Warren D. Seider
This processing strategy combines the advantages of batch and continuous operation, providing flexibility and efficiency in a single design.

Reduce Your Compressed Air Costs

October
2011
Fluids and Solids Handling
Ron Marshall, Bill Scales
Annual operating expenses for compressed air systems can exceed the equipment’s purchase price. Follow these seven steps to implement efficiency measures that yield cost reductions.

Designing Four-Pass Trays

April
2010
Back To Basics
Daniel R. Summers
Use this procedure to design four-pass distillation column trays and to balance the vapor/liquid ratio on each tray panel.

Take Another Look at Steam Traps

June
2001
Fluids and Solids Handling
S. Raghavi  Chari
Think twice before installing a steam trap. In the case of superheated lines, steam traps may prove to be a waste of time, effort, and money

Ease Control Valve Selection

November
2002
Fluids and Solids Handling
Kiran Nair, Liyakat Jaffer, Meredith Chapeaux, Sheetal Patel, Trevor Bishop
With so many types and options available, choosing the right control valve can seem daunting. Selection can be simplified by considering the process fluid, the service requirements, how the various valves function, and seeing how each valve will...

Steam Trap Troubles?

February
2005
Heat Transfer
Trinath Sahoo
First, prevent problems by selecting the appropriate trap and installing it properly. If problems arise, follow these guidelines for diagnosing and correcting them.

Selecting and Using Bolted Head Closures

April
2007
Fluids and Solids Handling
John C. Birkmire, P.E.
Proper design, fabrication, assembly and operation of a pressure vessel closure are essential to ensuring product containment, integrity and quality.

Don’t Let Baffle Tray Flood Baffle You

July
2011
Reactions and Separations
Henry Z. Kister, Matthew Olsson
Use this new correlation based on window liquid velocity to predict baffle tray capacity.

Optimizing Crystallizer Scaleup

June
2003
Fluids and Solids Handling
Wayne Genck
Explore how mixing parameters impact the crystallization process and recommend ways to improve the likelihood of successful scaleup. The concepts of nucleation and growth, types of mixing, design considerations, agitator parameters and scaleup...

Selecting Entrainers for Azeotropic Distillation

March
2009
Reactions and Separations
Madhura Chiplunkar, Vivek Julka, Lionel O’Young
This systematic methodology uses residue curve maps to identify and evaluate substances that can facilitate distillation by breaking an azeotrope.

Find Mixing Success through Failures - Part 1

October
2008
Fluids and Solids Handling
David S. Dickey, Gary K. Patterson
Understanding when and why mixing fails in the laboratory is often the only way of avoiding a similar failure in a production-scale reactor.

Guidelines for Crystallizer Selection and Operation

October
2004
Reactions and Separations
Wayne Genck
Continuous crystallizers serve a wide range of applications in the chemical process industries. Optimize system performance by heeding these practical design and operating principles, which apply to the forced circulation (FC), draft-tube-baffle (...

Efficient Technology Evaluation

February
2007
Critical Issues
Francesco Citro, Reuel Shinnar
To stay competitive in today's economic climate, rapid and effective assessments of new technologies is a must. Requiring a minimal amount of data, this powerful method can effectively evaluate new ideas and research programs at an early stage...

Screw Feeders: A Guide to Selection and Use

February
2003
Fluids and Solids Handling
Hermann J. Feise, Steven W. Couch, Thomas L. Krieger, Timothy Bell
Gain insight as to what screw feeder is best for your application. Plus, learn how to size, specify and test screw feeders.

Eliminate Iteration from Flow Problems

March
2008
Fluids and Solids Handling
John D. Barry
This article introduces a novel approach to solving flow and pipe-sizing problems based on two new dimensionless quantities that are independent of line size and flow.

Understand Thermodynamics to Improve Process Simulations

December
2011
Computational Methods
David Hill, Fred C. Justice, P.E.
Selecting a thermodynamic model is an important step in process simulation — one that many engineers overlook. This overview of applied thermodynamics can help you choose the right model for your process.

Optimize Pipeline Design for Non-Newtonian Fluids

March
2002
Fluids and Solids Handling
 Edgar Amaro  Ronces, Cinthya Alejandra Anguilar Guerrero, Alejandro Anaya Durand
Use this graphical method to determine pipe diameter, fluid temperature and pressure drop for laminar and turbulent flow.

Increase Powder Flow via Gas Injection

July
2006
Fluids and Solids Handling
John W. Carson, Herman Purutyan, Thomas G. Troxel
Fluidization and air-assisted discharge are two ways to optimize fine-solids handling. However, the choice of technology is as important as designing and operating the system properly.

Principles and Case Studies of Simultaneous Design

September, 2011
There are many comprehensive design books, but none of them provide a significant number of detailed economic design examples of typically complex industrial processes. Most of the current design books cover a wide variety of topics associated with process design. In addition to discussing...

Pump Wisdom: Problem Solving for Operators and Specialists

April, 2011
An accessible guide to the main reasons pumps fail—and what can be done about it Workhorses in many different industries, including the oil industry, water industry, chemical industry, food industry, and pharmaceutical industry to name a few, pumps are a vital contributor to maintaining and...

Teach Yourself the Basics of Aspen Plus

January, 2011
Aspen Plus is on of the most popular process simulation software programs used industrially and academically. Though the software is available at many corporations and universities, there are no textbooks which are dedicated to teaching the step-by-step use of the software. This book is designed to...

Reactive Distillation Design and Control

October, 2008
After an overview of the fundamentals, limitations, and scope of reactive distillation, this book uses rigorous models for steady-state design and dynamic analysis of different types of reactive distillation columns and quantitatively compares the economics of reactive distillation columns with...

Chemical Reactor Design, Optimization, and Scaleup, 2nd Edition

August, 2008
Chemical Reactor Design, Optimization, and Scaleup is the authoritative sourcebook on chemical reactors. This new Second Edition consolidates the latest information on current optimization and scaleup methodologies, numerical methods, and biochemical and polymer reactions. It provides the...

Chemical Reactor Design and Control

August, 2007
Chemical Reactor Design and Control uses process simulators like Matlab, Aspen Plus, and Aspen Dynamics to study the design of chemical reactors and their dynamic control. There are numerous books that focus on steady-state reactor design. There are no books that consider practical control systems...

Distillation Design and Control Using Aspen Simulation

April, 2006
As the world continues to seek new sources of energy, the distillation process remains one of the most important separation methods in the chemical, petroleum, and energy industries. And as new renewable sources of energy and chemical feedstocks become more universally utilized, the issues of...
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