(602ah) Fouling Rates of Synthetic Thin Stillage
AIChE Annual Meeting
2012
2012 AIChE Annual Meeting
Sustainable Engineering Forum
Poster Session: Sustainability and Sustainable Biorefineries
Wednesday, October 31, 2012 - 6:00pm to 8:00pm
Proteins,
carbohydrates, fats, ash and fiber in corn thin stillage are involved
in evaporator fouling. It is not understood which components
increase fouling rates. Costs associated with fouling include labor
and equipment needed to clean fouled heat transfer surfaces,
increased capital, antifoulant chemicals and production losses.
Effects of starch (STA) and glucose (GLU) composition in a synthetic
thin stillage fluid on fouling resistance (Rf)
were studied. Effects of total solids (TS) content (1 to 10% db) on
Rf
(m2K/kW)
was investigated. Synthetic thin stillage viscosity was measured
using a Rapid Visco Analyzer to determine the synthetic thin stillage
Reynolds Number (NRe). Fluid flow was turbulent (NRe
> 4000) for synthetic thin stillage with 1% TS and was constant,
irrespective of STA:GLU ratio. NRe
for synthetic thin stillage with 5 and 10% TS and having various
starch:glucose (STA:GLU) ratios was laminar (NRe
< 2100) and ranged from 500 to 1100. An annular probe was used to
measure fouling tendencies of synthetic thin stillage and Rf
was found at the end of 10 hr or until the probe temperature reached
170°C. Treatments with 1% TS, 10 hr long and STA:GLU composition
varying from 1:9 to 9:1 ratio had Rf range
of 0.254 to 0.303 m2K/kW. Synthetic thin stillage with STA only had Rf
range of 0.287 to 0.365 m2K/kW. Synthetic thin stillage with 5% TS and GLU only did not foul after
10 hr while 5% TS and STA only reached the maximum probe temperature,
170°C in 4.2 hr and had Rf
= 0.264 m2K/kW. Synthetic thin stillage with 10% TS and STA:GLU of 1:9 had
Rf = 0.163 m2K/kW
at the end of 10 hr but did not reach the maximum probe temperature,
170°C. As STA:GLU increased to 3:7, maximum probe temperature
was reached in 4.2 hr with final Rf
=
0.264 m2K/kW. Therefore, for 1, 5 and 10% TS, Rf
increased mainly because of the starch present in synthetic thin
stillage, while glucose had a smaller effect on Rf.
Higher concentrations of starch in synthetic thin stillage had
shortened the time to reach the maximum probe temperature.
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