Separations

Distillation in Practice

eLearning (online) Course
AIChE
This course covers all essential distillation concepts likely to be faced by process support, operations, and design engineering personnel.

Distillation Technology for Operators

eLearning (online) Course
AIChE
Operators will gain an excellent understanding of the theory of distillation and how it works in a column, plus gain a solid foundation on the...

Crystallization Process Development

eLearning (online) Course
AIChE
Integrative approach for crystallization development. Using models to analyze the SLE behavior of the system, validating using relevant experimental...

Impact of DDT on FPSO Explosion Risk Assessment

AIChE Spring Meeting and Global Congress on Process Safety
Apr 2, 2014
In recent explosion accidents on onshore petrochemical facilities, it has been concluded that a deflagration-to-detonation-transition (DDT) took...

Distillation in Practice

Instructor-led (classroom) Course
AIChE
This course covers all essential distillation concepts likely to be faced by process support, operations, and design engineering personnel. It covers...

Crystallization Operations

Instructor-led (classroom) Course
AIChE
Join crystallization expert Wayne Genck for a practical overview of the basics of crystallization and precipitation and how to apply the fundamentals...

Ten Distillation Revamp Pitfalls to Avoid

February
2014
Back To Basics
Doug Bouck
Projects aimed at improving distillation column operation may encounter a variety of hurdles. This article looks at ten common problems and provides guidance on how to avoid them.

Developing Crystallization Processes

March
2011
Reactions and Separations
Christianto Wibowo
With solid-liquid equilibrium as its foundation, this systematic approach makes it easy to identify operating regions and theoretical yield to maximize the desired product.

Understand the Basics of Membrane Filtration

April
2013
Back To Basics
Hongyi Zhou, Hua Wang
Membrane filtration is an integral part of many industrial processes, as it is often more environmentally sustainable and cost-effective than other separation technologies

New Materials for Membrane Separations

Mar 13, 2013
In this webinar, Dr. Richard D. Noble - the co-director of the NSF Industry/University Cooperative Research Center for Membrane Applied Science...

Realistically Predict Capacity and Pressure Drop for Packed Columns

July
2007
Reactions and Separations
Emil Abkar, Henry Z. Kister, Jeffrey Scherffius, Khashayar Afshar
Generalized pressure-drop correlation (GPDC) charts have been the standard for predicting packing flood points and pressure drops. This article guides engineers on the correct and incorrect uses of the GPDC interpolation procedure, and updates the...

Troubleshooting Distillation Simulation

June
2006
Reactions and Separations
Stanislaw K. Wasylkiewicz
A tool called azeotrope pressure sensitivity analysis (APSA) can shed light on the dependence of an azeotrope's composition and temperature on changes in pressure.

Understanding Crystallization and Crystallizers

October
2006
Fluids and Solids Handling
Ketan D. Samant, Lionel O'Young
Gain qualitative insight into the basic mechanisms of crystallization, the principles of crystallizer operation, and the ways in which these concepts relate to the selection and application of the various crystallizer configurations in industrial...

Diagnosing Maldistribution in Towers

May
2007
Reactions and Separations
Simon X. Xu
Gamma CAT-scan technology makes possible the collection of much more vital online process information than conventional diagnostic techniques.

Be Smart about Column Design

November
2012
Reactions and Separations
Daniel R. Summers, P.E., Mark Pilling, P.E.
Optimizing distillation equipment and processes can improve both the profitability and the greenness of an operation.

Distillation Troubleshooting

March, 2006
The last half-century of research on distillation has tremendously improved our understanding and design of industrial distillation equipment and systems. High-speed computers have taken over the design, control, and operation of towers. Invention and innovation in tower internals have greatly...

Solid-Liquid Separation: A Guide to Centrifuge Selection

July
2012
Back To Basics
Tom Patnaik
Centrifugation is a necessary step in many pharmaceutical and chemical production processes. These guidelines will help chemical engineers better understand the process of centrifuge selection.

CEP: AIChE Journal Highlight - A New Spin on Separations

September
2012
Journal Highlight
The microelectronics industry has been revolutionized by technologies that boast ever-increasing capabilities in increasingly smaller areas. Now, the ability to pack high functionality into smaller devices is poised to transform the chemical process...

Design and Control of Distillation Systems for Separating Azeotropes

March, 2010
Hands-on guidance for the design, control, and operation of azeotropic distillation systems Following this book's step-by-step guidance, readers learn to master tested and proven methods to overcome a major problem in chemical processing: the distillation and separation of azeotropes. Practical in...

Ionic Liquids

AIChE Webinar
Aug 26, 2009
This webinar will cover the use of Ionic Liquids for both liquid and gas separations, emphasizing how the choice of anion, cation and functional...

Oxygen and Nitrogen: Onward and Upward

January
2009
News Feature
Suzanne Shelley
Innovative advances continue to benefit all three of today's air separation technologies, helping to reduce power consumption and capital costs, and, in turn, expand their markets.

Using Chromatography to Separate Complex Mixtures

December
2010
Back To Basics
Nathalie Fraud
Purifying high-value mixtures, such as pharmaceuticals, can be an expensive undertaking. Choosing the correct chromatography methods can improve purity and reduce processing time and cost.

Converting a Commercial Distillation Column into a Research Tower

July
2005
Reactions and Separations
Ralph Weiland
Operating a column under actual distillation conditions is important for obtaining commercially valid hydraulic data. This article describes how a column was modified to operate in either a production or a research mode to collect hydraulic and mass...

Choosing Trays and Packings for Distillation

September
2009
Back To Basics
Bruce S. Holden , Mark Pilling
Tower-related problems can be difficult, time-consuming, and expensive to diagnose and fix. Here’s how to avoid difficulties and improve operating efficiency.

Improving Reverse Osmosis Performance

September
2010
Reactions and Separations
Loraine Huchler
Follow these guidelines for monitoring, evaluating, and troubleshooting RO units to ensure reliable and efficient system operation.

Optimize Energy Use in Distillation

March
2012
Reactions and Separations
Douglas C. White
Nonlinearities in the response of a column to changes in operating conditions and in common economic valuation functions can have significant impacts on the economic optimum energy consumption for the column. Here’s a way to account for such...

Get More Out of Single-Stage Distillation

February
2002
Reactions and Separations
Ernest A. Perkins , Ryan C. Schad 
Try these practical ways to boost capacity, increase product quality or reduce cycle time in batch and continuous systems.

Tools to Model Multiphase Separation

June
2007
Fluids and Solids Handling
David Connolly, Saeid Mokhatab, Timothy Newton
The flow fields in multiphase separators are often extremely complicated, making it difficult to model such systems. Computational fluid dynamics (CFD) and visual dynamic modeling (VDM) can be used together to overcome some of the challenges.

Reduce Costs with Dividing-Wall Columns

May
2002
Reactions and Separations
Dennis O'Brien, Douglas A. Stewart, James W. Harris, Michael A. Schultz, Mohamed S.M. Shakur, Steven P. Rosenblum
These distillation columns can significantly reduce capital and energy expenses vs. conventional multicolumn arrangements.

Clarifying Centrifuge Operation and Selection

August
2004
Fluids and Solids Handling
Victor Norton ,  William Wilkie
Before selecting a centrifuge for your application, understand its principles of operation and investigate the key process variables.

Select the Right Spray Nozzle

June
2001
Reactions and Separations
Peter  Welander, Terra L. Vincent
Finding the proper nozzle for specific applications doesn't have to be difficult. By applying basic concepts of nozzle technology, you can create a droplet profile that best suits your needs.

Troubleshooting Tangential Flow Filtration

June
2003
Reactions and Separations
Kent Iverson
Tangential flow filtration (TFF) is commonly used to concentrate and dialyze solutes. It generally involves the circulation of the feed solution over a filter surface. This article presents a brief overview of the principles governing TFF, and...

Visualizing the McCabe-Thiele Diagram

December
2009
Reactions and Separations
Paul M. Mathias
Use this spreadsheet-based visualization and interactive analysis of the McCabe-Theile diagram to understand the foundations of distillation engineering. <br><br>

Accurately Predict the VLE of Thiol-Hydrocarbon Mixtures

September
2004
Reactions and Separations
Chorng H. Twu, Vince Tassone, Wayne Sim
This methodology can be used to calculate vapor-liquid equilibria (VLE) between thiols and hydrocarbons at any composition, temperature or pressure to improve gasoline fractionation processes.

Bridge the Gap with Semicontinuous Distillation

August
2001
Reactions and Separations
James R. Phimister ,  Warren D. Seider
This processing strategy combines the advantages of batch and continuous operation, providing flexibility and efficiency in a single design.

Use Model-Predictive Control to Improve Distillation Operations

January
2008
Instrumentation
Daniel R. Webb, Robert D. Rounding, Robert J. Conroy, Umesh Mathur
This methodology, based on steady-state and dynamic simulation, can be used to develop the necessary models— and avoid disruptive and costly step testing to the extent feasible.

Real World Modeling of Distillation

July
2003
Reactions and Separations
Harry Kooijman, Rajamani Krishna , Ross Taylor
Previously, simulations based on nonequilibrium, or rate-based, models were considered impractical due to their complexity. However, with ever-increasing computing power, these simulations are not only feasible, but in some circumstances they should...

Don’t Let Baffle Tray Flood Baffle You

July
2011
Reactions and Separations
Henry Z. Kister, Matthew Olsson
Use this new correlation based on window liquid velocity to predict baffle tray capacity.

Squeeze More Out of Complex Columns

July
2002
Reactions and Separations
Piyush Shah
These distillation setups can cut capital and operating costs by up to 30%, and increase separation efficiency. Here is a straightforward method for evaluation.

Evaluating and Documenting Tower Performance

February
2010
Reactions and Separations
Daniel R. Summers
A good performance evaluation can lead to a significant improvement in column performance and establish a basis for future tower evaluations. <br>
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